High Pressure Stirred Lab Autoclaves / Reactors

High Pressure Parallel Autoclaves

Salient Features

  • High pressure autoclaves for chemical reactions like hydrogenation, oxidation, alkylation, chlorination. carboxylation, nitration, polymerization, amination, bromination,ethoxylation, esterification, sulphonation etc.
  • 50 ml to 100 liters volume
  • Pressures upto 350 bar & temperatures upto 500°C
  • Available in different Material of Constructions (MOC) like SS-316, SS-316L, Hastelloy B/C, Monel, Nickel, Inconel, Titanium, Tantalum, Zirconium
  • High torque zero leakage magnetic drive coupling
  • Ex-proof / CE / PED / ASME / UL / CSA certified systems on request
  • Fully automated PC controlled high pressure system / pilot plant to continuously monitor, control & record various parameters like temperature, pressure, motor speed, gas / liquid flow, level, pH, ORP, DO, IR, turbidity, torque etc.

Standard models for 10 ltr

Model no. A 3113 A 3115 A 3123 A 3125 A 3133 A 3135
Design Pressure100 bar200 bar350 bar
Design Temperature300°C500°C300°C500°C300°C500°C
Vessel I/D (mm)183
Vessel Internal Height (mm)420
Min. Stirrable Volume (ltr)1

Standard models for 20 ltr

Model no. A 3213 A 3215 A 3223 A 3225
Design Pressure100 bar200 bar
Design Temperature300°C500°C300°C500°C
Vessel I/D (mm)248
Vessel Internal Height (mm)495
Min. Stirrable Volume (ltr)2.6

Standard models for 25 ltr

Model no. A 3313 A 3315 A 3323 A 3325
Design Pressure100 bar200 bar
Design Temperature300°C500°C300°C500°C
Vessel I/D (mm)248
Vessel Internal Height (mm)595
Min. Stirrable Volume (ml)2.6

Standard models for 50 ltr

Model no. A 3403 A 3405 A 3413 A 3415
Design Pressure50 bar100 bar
Design Temperature300°C500°C300°C500°C
Vessel I/D (mm)355343
Vessel Internal Height (mm)558600
Min. Stirrable Volume (ml)6

Standard models for 100 ltr

Model no. A 3503 A 3505 A 3513 A 3515
Design Pressure50 bar100 bar
Design Temperature300°C500°C300°C500°C
Vessel I/D (mm)456440
Vessel Internal Height (mm)699735
Min. Stirrable Volume (ml)12

Note: The above ratings are only for SS316, Hastelloy C & Inconel materials, for other materials the ratings will change depending on its stress value & maximum allowable temperature as per ASME code.

Technical specification for 10 ltr 20 ltr, 25 ltr, 50 ltr & 100 ltr standard models

Sr. Description Specification
AMaterial of ConstructionSS 316 wetted parts
BHead Mounting StyleRemovable head and vessel design
CHeating TypeElectrical ceramic band heater with cladding & insulation & heater temperature control for 500°C
DMotor¼ hp AC motor for 10 ltr, 20 ltr & 25 ltr locked to 750 rpm
½ hp AC motor for 50 ltr & 100 ltr locked to 500 rpm
EShaft SealingZero leakage magnetic drive coupling M80 with 8 Nm torque for 10 ltr to 25 ltr & M120 with 12 Nm torque for 50 ltr & 100 ltr reactor
FStirrer2 stage 6 bladed turbine stirrer
GStandard Nozzles, Valves & FittingsExternal Valves & Fittings:
Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle valve with common dip tube, vent needle valve, ball valve for powder/liquid inlet with funnel, flush bottom valve
SizeNeedle valveBall valveFBV
10-25 ltr¼"¾"15mm
50 & 100 ltr½"1"25mm
Internal Fittings:
Helical cooling coil, dip tube, thermowell with RTD PT100 temperature sensor
HGasketPTFE up to 300°C and metallic grafoil gasket up to 500°C
IClosure TypeSplit clamp with clamp bolts
JControl PanelSS control panel with programmable PID temperature controller with high temperature alarm and variable frequency drive for motor speed control
KPower Supply1Ø, 220 V AC, 20 amp, 50 / 60 Hz for 10 ltr
3Ø, 440 V AC, 25 amp, 50 / 60 Hz for 20 ltr to 100 ltr
LMounting & DimensionsSS Trolley
Reactor VolumeDimensions with control panel in mm
WidthHeightDepth
10 ltr13105851550
20 ltr13105851700
25 ltr13105851800
50 ltr15006752350
100 ltr15007802350

Enquiry guide for 10 ltr, 20 ltr, 25 ltr, 50 ltr & 100 ltr customized high pressure autoclaves models

Enquiry code structure is Standard Model no-A-B-C-D1-D2-D3-E-F-G-I-J-L-M where A, B, C, D1, D2, D3, E, F, G, I, J, L & M options can be selected from below tables. The below options will be in place of standard supply. For example 100 ml, 100 bar, 300°C, Hastelloy C, fixed head autoclave with ATEX Zone1 certified, heater, motor & panel will read as A 1313-HC6-K-EZ-AZ-ATP

AMaterial of Construction
SS 316L316L
Hastelloy C 276HC6
Hastelloy C 22HC2
Hastelloy BHB
Monel BMN4
Inconel 600IN6
Inconel 625IN5
Nickel 200NK2
Titanium Gr. 2TI2
Zirconium 702ZR7
Tantalum linedTNL
BHead Mounting Style
Fixed head with pneumatic vessel raising lowering (10 ltr to 25 ltr)P
Fixed head with hydraulic vessel raising lowering (50 ltr & 100 ltr)H
Fixed head with pneumatic vessel raising lowering & tilting (10 ltr to 25 ltr)PT
Fixed head with hydraulic vessel raising lowering & tilting (50 ltr & 100 ltr)HT
CHeating Style
Electrical ex-proof, IIB + H2 certifiedEA
Electrical ex-proof ATEX Zone1 certifiedEZ
Electrical ex-proof Class 1 Div 2EC
Welded SS 304 jacket with insulationJS
Welded SS 304 jacket with electrical ceramic heaterJH
Limpet coil SS 304 with insulation (20 ltr to 100 ltr)LC
D1RPM
1 hpH10
2 hpH20
3 hpH30
D2RPM
Gear box upto 440 rpmR4
D3Motor Type
Ex-proof gas group IIB (Zone 1)XB
Ex-proof gas group IIC (Zone 1)XC
Ex-proof CE ATEX certified II 2G Ex de IIC T4AZ
Ex-proof CSA certified Class 1 Div 2 group A, B, C, DCD
¼ hp compact in-line brushless DC motorQD
EMag Drive Torque
12 Nm (for 10 to 25 ltr)M120
20 Nm (upto 750 rpm, for 10 to 25 ltr)M200
40 Nm(upto 750 rpm)M400
FStirrer Options*
Hollow shaft with gas induction ImpellerSH
Anchor (Serpentine cooling coil, max 100 rpm)SA
Spiral (No cooling coil, max 100 rpm)SS
Ruston turbineSR
PaddleSD
PropellerSP
GValves & Fittings
Serpentine cooling coilSCC
JControl Panel
Ex-proof gas group IIA/IIB zone 1 certifiedF2B
Ex-proof gas group IIC zone 1 certifiedF2C
Ex-proof ATEX zone 1 certifiedATP
Ex-proof class 1 div. 2 certifiedC12
Touch screenTSP
LMounting & Overall Dimensions (WxDxH) in mm
MountingVolumeReactor sizePanel sizeCode
Floor Stand10 ltr585 X 560 X 1550275 X 275 X 300FS
20 ltr585 X 560 X 1700400 X 380 X 340
25 ltr585 X 560 X 1800
50 ltr675 X 675 X 2350
100 ltr780 X 780 X 2350
MCertifications**
Design approval as per ASME code by notified bodyDAC
CE-PED 2014/68/EUPED
ASME U/U2 stamp codedASU
ATEX certified reactor 2014/34/EUASA
CE marked panel & electrical partsECE
UL/CSA marked panel & electrical partsUSC
Notes:
  1. Customer is advised to select best suited options for most optimized price & delivery.
  2. For other optional accessories please refer Accessories tab
  3. All above options may not be available / possible with all models.
  4. Customization of volume, material, pressure, temperature etc. of lab autoclaves may be possible on request.
  5. Different power supply options may be possible on request.
  6. Overall dimensions are indicative, they may change depending on the optional accessories or specific design modifications opted.
  7. * Stirrer options can be in place of standard or additional multiple interchangeable.
  8. ** Country specific certification like CRN for Canada, AS1210 for Australia & DOSH for Malaysia can be offered on request.

Lab Autoclaves Optional Accessories

Video

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