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Autoclave Optional Accessories

Gas Pressure Regulator
Gas Mass Flow Meter / Controller
Digital Pressure Indicator / Controller
Liquid / Gas charging High Pressure Pot
Ethylene Oxide Pot
Liquid Metering Pump System
Auto Cooling System
Low Temperature Cooling Bath
Reflux Condenser
Condenser
Receiver Pot
Oil Heating System
Jacket Flow Control Valves
Back Pressure Regulator
Data Logger
SCADA Software for Remote Operation & Recording
Catalyst Basket
Catalyst Filters
Catalyst Addition Device
Other Accessories

» Gas Pressure Regulator
To manually charge different gases at desired pressure upto 140 bar / Kg/cm² (2000 psi) or higher into the reactor from gas cylinder. Nitrogen, Oxygen & Hydrogen can be charged through same regulator(with special adaptor). Regulator for other gases like NH3, CO2 etc. can also be offered. The regulator comes with SS braided teflon high pressure hose pipe (4m long) non return valve (NRV), quick release coupling (QRC) & pressure gauges.
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» Gas Mass Flow Meter / Controller
Mass Flow Meters (MFM) can be used to measure the accurate mass flow rate of gas (in gm/hr or / LPH) & totalised quantity of mass (in gms/ Litr.) charged in autoclave at any point. Mass flow controller (MFC) is used to charge the set flow rate of gas into the autoclave at high pressures up to 350 bar / Kg/cm² or it can be used in pressure control mode to indicate the gas flow & total flow to maintain desired set pressure inside the autoclave. The same MFM / MFC can be used for mutiple gases by just entering the conversion factor for different gas densities provided the gases are inert to each other. The MFM/MFC comes with high pressure flexible hose, inlet filter NRV & QRC with digital gas flow indicator cum totaliser & additional pressure PID controller with pressure sensor if the MFC is used in pressure control mode. User has to specify the max. flow rate range, pressure & gas for ordering MFM/MFC.
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» Digital Pressure Indicator / Controller
It consists of pressure sensor (transmitter) & digital pressure indicator/ controller (mounted on common control panel) with pressure alarm & optionally heater cut off for safety. Digital pressure indicator has pressure reading in bar or kg/cm² & psi. where as controller reads any one of the 3 units. The controller is normally used with mass flow controller (MFC) to maintain constant pressure inside the autoclave. With MFC, gas flow indication & totaliser are also provided on the same panel. The pressure sensor has temperature limitation upto 80ºC & hence the same is provided with water cooling jacket. optionally intrinsically safe pressure sensor with IIC certification is provided. Pressure sensor with Hastelloy C-276 wetted parts be offered on request.
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» Liquid / Gas Charging High Pressure Pot
It is used to transfer liquid or gases in to the autoclave under pressure. It consists of high pressure SS-316 pot designed for working pressure 100bar/ kg/cm² or higher with port for Nitrogen gas (N2) pressure, liquid inlet, liquid outlet, pressure gauge, high pressure hose, QRC, & NRV. The liquid to be charged is fed into the pot from top funnel & pressurised with N2 gas until its pressure is higher than the autoclave pressure & then under pressure the liquid is charged into the autoclave. The quantity & rate of flow of liquid charged is not known precisely in this system. Pots of different pressure, M.O.C. & sizes can be offered. This pot also be used for storage of gases when gas cylinders are far off.
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» Ethylene Oxide Pot
It consist of SS-304/316 ethylene oxide horizontal pot with inlet, outlet, gas inlet with dip tube, thermowell & pressure gauge for 10kg/cm2 working pressure. It is used for ethoxylation.
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» Liquid Metering Pump System
This system is used to charge the liquid at desired rate from as low as 1ml/hr. To 100Ltr./hr, when the autoclave is under pressurised condition. The metering system comes with pump, flow controller, liquid sump, pressure safety valve, pressure gauge, strainer, high pressure hose, NRV & QRC. Optionally flow totalizer is also provided. AMAR offers 2 types of pumps.
(a) Low cost Diaphgram pumps for pressure upto 100 bar & min. flow range upto 60-600ml/hr. to max. 10-100 lit/hr. The flow rates are varied by varying the motor speed with variable frequency drive.
(b) HPLC type low flow metering pumps for high pressures upto 350 bar & min. flow range upto 0.6 to 300ml/hr.
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» Auto Cooling System
The control panel of the autoclave gives 230V, 1Ø or 3Ø 415V (optionally) output to connect external auto-cooling system. AMAR gives 2 options:
(a) Solenoid valve (Flameproof / non-FLP) connected at the inlet of the internal cooling coil with external source of chilled water supply. This is standard for 50ml & 100ml autoclaves, However for bigger autoclaves if the cold water line pressure is <2bar then it is better to opt for external pump & tank water cooling system. Normal tap water cooling is not effective at higher temperature due to steam back pressure whereas auto cooling system gives positive pump pressure.

(b) Pump & Water Cooling Tank: This system is used to control the overshoot in the autoclave & to cool it rapidly to lower temperature after the reaction is over. It circulates water to the internal cooling coil of reactors. It is a very essential feature for highly exothermic or runaway reactions. Cooling starts automatically if the rate of heating rises suddenly. It comes with ½ H.P monoblock/ FLP II & IIB/ IIC coupled pump, tank, pipeline & flexible hose pipes with QRC & is mounted on the autoclave trolley itself.

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» Low Tempereature Cooling Bath
It is used to reduce the autoclave temp. to as low as upto -50 deg.C from room temperature to carry out reactions at lower temp. It consist of single/double stage compressors, expansion valve, condensor, stirrer, circulation pump with control panel to control the temp. of the media in bath.Cooling media/oil is cooled in the bath and then circulated to the internal coil/jacket of the autoclave through 6ft. Flexible silicon/SS hoses with insulation.
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» Reflux Condenser
It is a jacketed tube SS-316 (0.02m² area) heat exchanger used to reflux the condensate back into the reactor & vent off the uncondensed vapours. It works under full autoclave pressure. Reflux condenser can be offered in different MOC & area.
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» Condenser
It is a SS-316 shell & tube reverse flow heat exchanger for distillation/condensing the vent vapours from the autoclave upto 10Kg/cm² pressure. It can be offered in all different MOC, higher pressure & different surface areas from 0.1m2 to 2m². The condensate can be collected separately or optionally refluxed back into the reactor.
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» Receiver Pot
Receiver Pot can be connected at the outlet of the shell & tube or Reflux condensor to collect the condensate separately. It is also provided with port to apply vacuum & offered in 1/2L to 5L sizes. Higher sizes & MOC can be offered on special request.
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» Oil Heating System
It is opted only if heating is jacket type & the area is totally flameproof or direct electric band heaters are not permissible. Heating can be done by circulating hot oil through the jacket of the autoclave. The system comes with SS tank (15-45L capacity depending on autoclave volume) with electric heaters, level switch, pump, temperature controller with alarm system & 6ft SS braided flexible hoses with insulation. Heating bath can be placed at a distance. Standard system have max. bath temp. 250ºC & autoclave temp. 225ºC & suitable only upto 100L autoclaves. Oil bath for higher temp. upto 300ºC can be quoted on request. Thermic oil for high temp. can also be supplied along with the bath.
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» jacket flow control valves
These valves can be connected at jacket inlet for controlling flow of steam/ hot oil/ water for temperature control from PID. Amar gives 2 options

(a) On/off electro pneumatic ball valve actuated by 230V output from panel to solenoid valve inline of air supply

(b) Pneumatic or proportionate flow control/ valves with I to P Convertor (for accurate temperature control).
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» back pressure regulator
It is mounted on the ventline of the autoclave & is used for maintaining constant pressure inside the autoclave. The pressure is maintained by releasing the excess pressure into the atmosphere or through a hose to safe area. The pressure can be set initially on the gauge, by manually varying the knob until the gas comes out. Once the set pressure is exceeded the excess pressure is released until the autoclave pressure becomes equal to or below the set pressure. The pressure release is slow & gradual & the set pressure can be varied at any point. Alternately electronic digital back pressure regulator can be offered on request.
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» data logger
It is used for recording temp. Pressure, RPM etc. process & set values with provision to take online or offline printing (in serial port printer) / data transfer on PC with RS485/232 convertor.
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» scada software for remote operation & recording
It consist of a software with all controllers / indicators having RS485 communication port, for online display, set point changes & data logging of pressure, temp., Motor RPM & optionally liquid / gas flow rate with totaliser etc. remotely from PC as well as locally from panel. It gives continuous online data logging at predefined variable time interval, online graphical representation as well as historical data on PC. RS-485-232 convertor & cable upto 10m or higher is also supplied.
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» Catalyst Basket
It is provided to improve the efficiency of the catalysts & for holding the catalyst so that it will not be destroyed or changed by the stirring action of impeller. The baskets are made from SS wire mesh & connected to the stirrer so that it rotates with the stirrer. It is available for 400ml-2Ltrs. autoclave.
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» Catalyst Filters
These are small 2 or 5 microns sintered disc filters which are connected at bottom of the sampling dip tube so that while sampling liquid, the catalyst does not come out. It is very good system since the catalyst is normally very expensive or pyrophoric. These filters may reduce the rate/ flow of the sampling liquid due to the resistance offered by the fine mesh, filters are available for 400ml-100Ltrs. Autoclaves
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» Catalyst Addition Device
It is used for charging catalyst under pressure during the reaction. It consists of a 5ml to 20ml (depending on Autoclave size) small container with airtight cap, that is openable. The powder is filled in the container which is then threaded to the autoclave head from below to a separate port with needle valve on the top. Under atmospheric & pressurized conditions the powder remains inside the container as the cap remains closed. One has to apply gas pressure greater than autoclave pressure from the needle valve on that port so that the cap opens & releases the catalysts inside the autoclave under pressure. Depending on the optional accessories selected, sometimes the catalyst addition device may not be possible due to space constraint on the head.
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» Other Accessories
Level sensors

pH/ DO/ ORP/ Redox sensors

Removable baffles in small autoclaves for better stirring

Serpentine cooling coils when material is sticky & difficult to clean — — — — — — — — — — — — — — — — — — — — —>

View glass/ windows to see the reactions
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Gas Pressure Regulator
Gas Mass Flow Meter / Controller
Digital Pressure Indicator / Controller
Liquid / Gas charging High Pressure Pot
Ethylene Oxide Pot
Liquid Metering Pump System
Auto Cooling System
Low Temperature Cooling Bath
Reflux Condenser
Condenser
Receiver Pot
Oil Heating System
Jacket Flow Control Valves
Back Pressure Regulator
Data Logger
SCADA Software for Remote Operation & Recording
Catalyst Basket
Catalyst Filters
Catalyst Addition Device
Other Accessories